Gamry Multi-purpose Corrosion Measurement Cell Set

Product archive | Electrochemistry accessories, Gamry Instruments | Topic: Gamry Accessories Electrochemistry
CorrosionElectrochemical impedance spectroscopyElectrochemical Instrumentation
The design of the multi-purpose corrosion cell set not only makes cleaning easy but also offers a high degree of flexibility for electrochemical corrosion experiments involving a wide range of specimen geometries

The multi-purpose corrosion cell set has been designed for ease of use, reliability and easy cleaning. In addition to electrochemical corrosion experiments at a constant temperature, the optional heating and cooling jacket also enables temperature-dependent investigations to provide a better understanding of the heterogeneous redox reaction system in a 1000 ml volume of electrolyte.

Product Description

The high flexibility of the Multipurpose Corrosion Cell Set allows either custom specimen geometries using the removable top plate or the included Alabama Specialty Products working electrode and compatible geometries for the optional Flat Specimen Holder. Made of Pyrex®, the multi-purpose corrosion cell set has a total of seven connections. Three glass sleeves with an internal thread from ACE GLASS INC. Vineland / NJ ( #7 Ace Thread), three 24/40 ground glass sleeves and one SJ 28/15 spherical ground glass dish.

The vertical 24/40 ground glass sleeve in the centre accommodates an adapter for a glass tube in the middle of which the working electrode can be screwed on with a threaded rod. To ensure that only the working electrode and not the metal threaded rod comes into contact with the electrolyte, two Teflon sealing elements are provided above and below the glass tube, which are locked against the working electrode with a nut.

A further 24/40 ground joint sleeve is used to accommodate an inert gas supply for rinsing via a nozzle tube with frit or as a shielding gas supply. The third 24/40 ground joint sleeve serves as a reserve, for example for adding reagents or for venting.

The side SJ 28/15 spherical ground joint shell accommodates an adapter for a curved Luggin capillary for use with a Gamry reference electrode, which is held in the Luggin capillary via the single #11 Ace thread with the corresponding threaded bushing.

The range of movement of the spherical ground joint and the curved Luggin capillary ensure a very small adjustable distance between the working and reference electrodes. One or two graphite counter electrodes can be attached to the #7 Ace Threads for a more even current distribution. A further #7 Ace thread serves as a reserve for temperature measurements in bulk or also for venting.

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The Gamry Interface 1010 Potentiostat Starter Pack

Specifications

DIMENSIONS



Ø15 cm x 42 cm (H) – Standard version

Ø21 cm x 45 cm (H) – Version with heating/cooling jacket




SYSTEM


Material: Pyrex®, PTFE, Vycor glass, ACE FETFE, graphite, polyethylene



Type:

Glass vessel with and without heating/cooling jacket

Lid plate (3x NS14/20, 3x #7 Ace – Thread, 1x SJ 15/28 ball socket)



Volume: 1000 ml



CONFIGURATION



Working electrode connection (type) 24/40 ground sleeve

Working electrode connection (Ø / mm) 7 – 9

Working electrode connection (L / cm) 8

Working electrode area (cm²) 5



Flat specimen holder connection (type) PEEK / Centring piece / NS 24/40

Maximum specimen thickness (mm) 7

Round working electrode (Ø / mm) 25 – 30

Rectangular working electrode max. 23 x max. 23

Exposed working electrode (Ø / mm) 10

Working electrode area (cm²) 0.785

Temperature resistance up to max. (°C) 80



Luggin capillary connection (type) SJ 15/28 ball joint

Luggin capillary / electrolyte contact Vycor® disc Ø, 3.5 mm

Reference electrode connection (type) #11 Ace – Thread

Reference electrode connection (Ø / mm) 9 – 11.5



Counter electrode connection (type) #7 Ace – Thread

Counter electrode 300 mm graphite rod / Ø 6.3 mm



Inert gas purge connection (type) 24/40 sleeve

Inert gas purge
24/40 core (purge / feed or vent)


Additional connection (type) 1x 24/40 sleeve / 2x #7 Ace – Thread



Options and Accessories

• Interface 1000 Potentiostat/Galvanostat/ZRA

Interface 1010 Potentiostat/Galvanostat/ZRA

• Reference 600 Potentiostat/Galvanostat/ZRA

Reference 600+ Potentiostat/Galvanostat/ZRA

Reference 3000 (AE) Potentiostat/Galvanostat/ZRA

• Flat Specimen Holder

• MultiPort Corrosion Cell Kit, Standard (excludes reference electrode)

• MultiPort Corrosion Cell Kit, Jacketed (excludes reference electrode)

• 24/40 Teflon adapter for glass electrode holder

• Graphite Rod, Counter Electrode – 12 inches

• Teflon gasket for sample rod

• Centring Washer for Sample Rod

• C1018 mild steel sample

• Cylindrical specimen support rod

• Hex nut for sample rod, stainless steel

• Gas dispersion tube for multiport corrosion cell

• SJ 28 male to #7 Ace thread adapter

• Glass tube for cylindrical electrode holder

• Multiport corrosion cell 7-neck top

• Multiport corrosion cell bottom, standard

• MultiPort Corrosion Cell bottom, jacketed

• Reference bridge tube for MultiPort corrosion cell

• Flexcell CPT Clamp, 4″ Shot Flange

• Corrosion Cell Flat Specimen Holder

• #7 Ace-threaded bushing with O-ring

• #11 Ace-threaded bushing with O-ring

• Ball Joint Clamp SJ28

• #7 Ace-thread plug, nylon, front seal (incl. FETFE O-ring)

• Stopper 24/40, polyethylene

• O-ring, Teflon-encapsulated silicone

• Calomel (SCE) reference electrode

• Silver/silver chloride reference electrode

• Mercury sulphate reference electrode (without chloride anions)

• Mercury oxide reference electrode for alkaline media

• Silver/silver nitrate reference electrode for non-aqueous electrolytes

• SCE refill solution (120 ml)

• Ag/AgCl refill medium (120 ml)

• Vycor frit with Teflon heat-shrink tubing, 3.5 mm (5 pieces)

• KT glass frit with Teflon heat-shrink tubing, 3.5 mm (5 pieces)

• Polymer exchange frits for mercury oxide reference electrode

Applications