Gamry UV-VIS-NIR Spectroelectrochemistry

Product Description

The coupling between electrochemistry and spectroscopy is very valuable for elucidating the redox behaviour of polymers, transition metals, metal and organometallic complexes, biological interface systems or electroactive functional layers.

Gamry’s spectroelectrochemical system includes various spectrometers from UV/VIS (Exemplar series) to NIR (Sol series), a light source with deuterium / tungsten halogen lamp, a wide range of fibre optic cables and a 2-/3-way cuvette holder for absorption, transmission or fluorescence measurements at room temperature. If you need to work under inert gas, you also have the option of choosing the appropriate cuvette holder with the simultaneous option of temperature control from -30°C to 150°C.

Optical components are very sensitive to contamination. The service life, quality and reproducibility of measurements can suffer as a result. The spectrometer, light source and cuvette holder are therefore fitted with metal sealing caps to protect them from dust and contamination. The fibre optic cables also have plastic dust and dirt protection caps. Ideally, these protective caps should only be removed for the experiment and then replaced. When assembling a spectroelectrochemical experiment, gloves are also required to avoid irreversible deposits in the event of direct contact.

Another necessity for spectroelectrochemical measurements are special connection cables for the often very sensitive working and counter electrode connections. We therefore always supply the appropriate extension cable for your spectroelectrochemical setup.

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Specifications

SPECTROMETER (Sample; recommended)



Dimensions: 5.7 cm (W) x 8.7 cm (L) x 3.4 cm (H)

Smart CCD array: 2048 pixels

Pixel size: 14 µm x 200 µm

Grating: 600 lines/mm, Blaze-λ 400 nm

Slit width: 10 µm

λ range: 350 nm – 1050 nm

Resolution: 1 nm



SPECTROMETER (Sol 1.7; recommended)


Dimensions: 10.9 cm (W) x
19.5 cm (L) x 6.8 cm (H)

NIR TE-cooled InGaAs CCD array: 512 pixels

Pixel size: 25 µm x 500 µm

Grating: 150 g/mm, Blaze-λ 1250 nm

Slit width: 25 µm

λ range: 900 nm – 1700 nm

Resolution: 4 nm



LIGHT SOURCE



Dimensions: 18.7 cm (W) x 27.6 cm (L) x 13.0 cm (H)

Light sources: Deuterium (UV) / Tungsten (VIS/NIR)

Spectral range: 190 nm to > 2500 nm

Manual control / triggering of the spectral range and ‘shutter’

UV spectral range: 185 nm – 400 nm

VIS/NIR spectral range: 400 nm – 2500 nm.



CUVETTE HOLDER


Dimensions: 5.1 cm (W) x
6.3 cm (L) x 7.5 cm (H)

Spectral range: 190 nm – 2100 nm

Application: 2-way (absorption and transmission; BCH100A), 3-way (absorption, transmission and fluorescence; BCH103A)

Connections: SMA 905 incl. collimator optics


FIBRE
OPTIC CABLE



SMA905 with 600 µm diameter and 0.22 NA (numerical aperture) required

Options and Accessories

• Interface 1000 Potentiostat/Galvanostat/ZRA

• Interface 1010 Potentiostat/Galvanostat/ZRA

• Reference 600 Potentiostat/Galvanostat/ZRA

• Reference 600+ Potentiostat/Galvanostat/ZRA

• Reference 3000 (AE) Potentiostat/Galvanostat/ZRA

Measurement cells and accessories:

• Vista Shield Faraday Cage

• Reference electrodes

• Spectroelectrochemistry Cell Kit

• Cuvette lid for spectroelectrochemistry

• Pt mesh WE for Spectroelectrochemistry

• Standard quartz cuvette, 10 mm path length

• ITO Electrode Spectroelectrochemistry Cell Kit

• Standard quartz cuvette, 10 mm path length

• Pt wire counter electrode

• ITO cuvette lid set

• ITO substrate set (sheet resistance 10 Ω – 15 Ω, polished float glass, 8 mm x 60 mm, 1.1 mm thick) including two connectors

 

Applications